| Individual course details | ||||||||||
| Study programme | Computer and applied physics | |||||||||
| Chosen research area (module) | Metrology | |||||||||
| Nature and level of studies | Undergraduate studies | |||||||||
| Name of the course | Measuring - Instrumental Techniques | |||||||||
| Professor (lectures) | Rastko Vasilic | |||||||||
| Professor/associate (examples/practical) | Rastko Vasilic | |||||||||
| Professor/associate (additional) | Rastko Vasilic | |||||||||
| ECTS | 4 | Status (required/elective) | required | |||||||
| Access requirements | none | |||||||||
| Aims of the course | Instrumental analysis/techniques for studying solids introductory course | |||||||||
| Learning outcomes | Students are able to identify and partially operate characterization techniques that are often found in scientific labs. | |||||||||
| Contents of the course | ||||||||||
| Lectures | 1. Intorduction: types and classification of instrumental analysis methods. 2. Optical spectroscopy: components of optical instrumentation, sources of radiation, wavelength selectors, detectors. UV-Vis-NIR molecular spectroscopy: quantitative aspect of absorption measuremen, instrumentation for absorption measurement, practical applications. 4. Diffuse reflectance spectroscopy. 5. Fluorescence, phosphorescence and chemiluminescence: principles and instrumentation. 6. Atomic absorption spectroscopy (flame and electrothermal atomization). 7. Infrared absorption spectroscopy: theory, IR sources and detectors, IR devices. 8. Raman spectroscopy. 9. NMR spectroscopy. 10. X-ray spectroscopy: fluorescence, diffraction, and absorption. 11. Mass spectroscopy. 12. Ellipsometry. 13. Electron emission spectroscopy. 14. Scanning and transmission electron microscopy. Scanning probe microscopy. | |||||||||
| Examples/ practical classes | Laboratroy excersies/demonstration are following lectures. | |||||||||
| Recommended books | ||||||||||
| 1 | D.A. Skoog, F.J. Holler, T.A. Nieman, Principles of instrumental analysis, 5th ed, BrooksCole, 1998 | |||||||||
| 2 | V. Jokanovic, Instrumental methods - a key for understanding nanotechnology, Albos, 2014 | |||||||||
| 3 | S. Mentus, Lj. Damjanovic, Physicho-chemical analysis, Faculty of physical chemistry, 2015 | |||||||||
| 4 | Y. Leng, Materials characterization-introduction to microscopic and spectroscopic methods, John Wiley & Sons (Asia) Pte Ltd, 2008. | |||||||||
| 5 | ||||||||||
| Number of classes (weekly) | ||||||||||
| Lectures | Examples&practicals | Student project | Additional | |||||||
| 2 | 2 | 1 | ||||||||
| Teaching and learning methods | Lectures, laboratory excersies / demonstrations, hands-on experience | |||||||||
| Assessment (maximal 100) | ||||||||||
| assesed coursework | mark | examination | mark | |||||||
| coursework | 10 | written examination | 40 | |||||||
| practicals | 10 | oral examination | 10 | |||||||
| quizzes | 10 | |||||||||
| mid term exam | 20 | |||||||||